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HRID615425

反应详情

EQUATION

反应方程式

HRID 615425 反应方程式

REACTANTS

反应物

3
Methacryloyl chloride 分子结构式
HCID13528

Methacryloyl chloride

C4H5ClO

1,4-Dioxane 分子结构式
HCID31275

1,4-Dioxane

C4H8O2

12-Aminododecanoic Acid 分子结构式
HCID69661

12-Aminododecanoic Acid

C12H25NO2

PRODUCTS

产物

1
12-[(2-Methylacryloyl)amino]dodecanoic acid 分子结构式
HCID19386585

12-[(2-Methylacryloyl)amino]dodecanoic acid

C16H29NO3

收率 73%

AUXILIARIES

试剂、催化剂与溶剂

1
Water 分子结构式
溶剂HCID962

Water

H2O

PROCEDURE

实验过程

0.3 Mole of methacrylic acid chloride and 0.3 mole of 12-aminododecanoic acid were reacted in a mixed solvent of dioxane and water under Schotten Baumann reaction conditions to obtain N-methacryloyl-12-aminododecanoic acid in a yield of 73%.