huagongshe.com
HRID615500

反应详情

EQUATION

反应方程式

HRID 615500 的结构方程式

REACTANTS

反应物

3
结构：CI
HCID6328

Methyl iodide

CH3I

结构：O=C([O-])[O-].[K+].[K+]
HCID11430

Potassium Carbonate

CK2O3

结构：COC(=O)c1cc(O)c(C)cc1Br
HCID20428674

未命名化合物

PRODUCTS

生成物

1
结构：COC(=O)c1cc(OC)c(C)cc1Br
HCID20428669

Benzoic acid, 2-bromo-5-methoxy-4-methyl-, methyl ester

C10H11BrO3

AUXILIARIES

试剂、催化剂与溶剂

1
结构：CC(C)=O
溶剂HCID180

Acetone

C3H6O

PROCEDURE

实验过程

A mixture of 800 mg of material from step b. 10 ml of dry reagent grade acetone, 456 mg of K2CO3, and excess methyl iodide was stirred a refluxed for 3 days. Ether extraction provided the ester in a form suitable for further transformation.

WORKUP

后处理

  1. temperaturea refluxed for 3 days
  2. extractionEther extraction