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HRID615695

反应详情

EQUATION

反应方程式

HRID 615695 的结构方程式

REACTANTS

反应物

3
结构：CCOC(=O)C(C#N)NC(C)=O
HCID95422

Ethyl 2-(acetylamino)-2-cyanoacetate

C7H10N2O3

结构：CC[O-].[Na+]
HCID2723922

Ethanol, sodium salt

C2H5NaO

结构：BrC1Cc2ccccc2C1
HCID10965463

2-BROMOINDAN

C9H9Br

PRODUCTS

生成物

1
结构：CCOC(=O)C(C#N)(NC(C)=O)C1Cc2ccccc2C1
HCID13517005

未命名化合物

AUXILIARIES

试剂、催化剂与溶剂

1
结构：CS(C)=O
溶剂HCID679

Dimethyl sulfoxide

C2H6OS

2 次

PROCEDURE

实验过程

Sodium ethoxide (40 gms) was stirred in 1 L of dimethyl sulfoxide until solution was complete. Then, 100 g of ethyl acetamido-cyanoacetate was added, and again stirred until solution was complete. 2-Bromoindane (101 g) was slowly added, using a few ml of DMSO to wash the container and addition funnel. The solution was stirred over a weekend.

WORKUP

后处理

  1. washto wash
  2. additionthe container and addition funnel
  3. stirringThe solution was stirred over a weekend