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HRID616370

反应详情

EQUATION

反应方程式

HRID 616370 的结构方程式

REACTANTS

反应物

3
结构：CC(C)N(CCCl)C(C)C.Cl
HCID77942

N-(2-chloroethyl)-N-(propan-2-yl)propan-2-amine hydrochloride

C8H19Cl2N

结构：[Na]
HCID5360545

Sodium

Na

2 次

结构：CCCCOc1ccccc1O
HCID12447746

2-Butoxyphenol

C10H14O2

PRODUCTS

生成物

1
结构：CCCCOc1ccccc1OCCN(C(C)C)C(C)C
HCID3042672

N-[2-(2-Butoxyphenoxy)ethyl]-N-(propan-2-yl)propan-2-amine

C18H31NO2

AUXILIARIES

试剂、催化剂与溶剂

1
结构：CCO
溶剂HCID702

Ethanol

C2H6O

2 次

PROCEDURE

实验过程

To 750 ml of absolute ethanol was added gradually 13.8 g (0.60 mole) of metallic sodium cut into pieces. After all the sodium had reacted 49.8 g (0.30 mole) of o-butoxyphenol was added. The solution was cooled down in ice-water whereupon a solution of 60.0 g (0.30 mole) of diisopropylaminoethylchloride hydrochloride in 150 ml of absolute ethanol was added rapidly with stirring. The reaction mixture was then boiled under reflux for 5 hours.

WORKUP

后处理

  1. additionwas added
  2. additionwas added rapidly
  3. temperatureunder reflux for 5 hours