HRID616671

反应详情

EQUATION

反应方程式

HRID 616671 的结构方程式

AUXILIARIES

试剂、催化剂与溶剂

3

PROCEDURE

实验过程

In the manner given in Example 1, a solution of 9-trifluoromethyl-1-methyl-6-phenyl-4H-s-triazolo[4,3-a][1,4]benzodiazepine in dimethylformamide, N,N,N',N',-tetraethyldiaminomethane and acetyl bromide (in 0.2 molar excess compared to the N,N,N',N'-tetraethyldiaminomethane) are reacted together to give 9-trifluoromethyl-1-[2-(diethylamino)ethyl]-6-phenyl-4H-s-triazolo[4,3-a][1,4]benzodiazepine.

WORKUP

后处理

  1. customare reacted together