Triethylamine → HCID 21849028, compound

HRID 617689Notes

Reaction equation

HRID 617689 reaction equation
[CH:1]1[CH:6]=[C:5]2[C:7]([Cl:12])=[N:8][S:9](=[O:11])(=[O:10])[C:4]2=[CH:3][CH:2]=1.[CH2:13]([N:15]([CH2:18][CH3:19])[CH2:16][CH3:17])[CH3:14]>CC(C)=O>[Cl-:12].[CH2:13]([N+:15]([CH2:18][CH3:19])([CH2:16][CH3:17])[C:7]1[C:5]2[CH:6]=[CH:1][CH:2]=[CH:3][C:4]=2[S:9](=[O:11])(=[O:10])[N:8]=1)[CH3:14]

Participants

4

Reactant 2

HCID 8471TriethylamineHCID 64783Pseudosaccharin chloride

Product 1

HCID 21849028HCID 21849028, compound

Reagents, catalysts & solvents 1

HCID 180AcetoneSolvent

Procedure

10.0 g of pseudosaccharine chloride are dissolved in 40 ml of acetone, and 5.1 g of triethylamine (diluted with 5 ml of acetone) are added. The reaction temperature is held at room temperature by ice cooling. After stirring for 10 hours, the resultant precipitate is isolated to give 5.3 g (35%) of 3-triethyl-ammoniobenzoisothiazole 1,1-dioxide chloride.

Workup

  1. customis held at room temperature by ice cooling

Sources & evidence

ORD record
ord-f752e0f6675f4f62913c0fedae76f1bd
Source dataset
uspto-grants-1999_09
Patent number
US05952282

Reaction notes

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