2-Methoxyethylamine → HCID 178496015, compound

HRID 620442Notes

Reaction equation

HRID 620442 reaction equation
CO[C:3]([C:5]1[NH:9][N:8]=[C:7]([N+:10]([O-:12])=[O:11])[N:6]=1)=[O:4].[CH3:13][O:14][CH2:15][CH2:16][NH2:17]>O1CCOCC1>[CH3:13][O:14][CH2:15][CH2:16][NH:17][C:3]([C:5]1[NH:9][N:8]=[C:7]([N+:10]([O-:12])=[O:11])[N:6]=1)=[O:4]

Participants

4

Reactant 2

HCID 80182-MethoxyethylamineHCID 178499123HCID 178499123, compound

Product 1

HCID 178496015HCID 178496015, compound

Reagents, catalysts & solvents 1

HCID 312751,4-DioxaneSolvent

Procedure

To 1 g of 3-nitro-1,2,4-triazole-5-carboxylic acid methyl ester dissolved in 5 ml of dioxane is added 1 g of methoxy ethylamine. The reaction mixture is warmed at 40°-50° C. for 2 hr with stirring.

Workup

  1. temperatureThe reaction mixture is warmed at 40°-50° C. for 2 hr

Sources & evidence

ORD record
ord-378634633b1e4c90807cc3193305b946
Source dataset
uspto-grants-1989_04
Patent number
US04820844

Reaction notes

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