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HRID621458

反应详情

EQUATION

反应方程式

HRID 621458 的结构方程式

REACTANTS

反应物

4
结构：Cl
HCID313

Hydrochloric Acid

ClH

结构：c1ccc2c(c1)CCNCC2
HCID1400243

2,3,4,5-Tetrahydro-1H-benzo[d]azepine

C10H13N

结构：CC(=O)N1CCc2ccc(S(C)(=O)=O)cc2CC1
HCID11265634

未命名化合物

结构：CC(=O)N1CCc2ccc(S(=O)(=O)Cl)cc2CC1
HCID11346737

3-acetyl-7-chlorosulfonyl-2,3,4,5 -tetrahydro-1H-3-benzazepine

C12H14ClNO3S

PRODUCTS

生成物

1
结构：CS(=O)(=O)c1ccc2c(c1)CCNCC2.Cl
HCID21242879

未命名化合物

PROCEDURE

实验过程

Following the procedure of Examples 1 and 4, 2,3,4,5-tetrahydro-1H-3-benzazepine was converted to 3-acetyl-7-chlorosulfonyl-2,3,4,5-tetrahydro-1H-3-benzazepine and then to 3-acetyl-7-methylsulfonyl-2,3,4,5-tetrahydro-1H-3-benzazepine which was hydrolyzed with hydrochloric acid to give 7-methylsulfonyl-2,3,4,5-tetrahydro-1H-3-benzazepine hydrochloride, m.p. 275°-277° C.