Potassium Carbonate → HCID 19858315, compound

HRID 621501Notes

Reaction equation

HRID 621501 reaction equation
[CH3:1][O:2][CH:3]=[CH:4]C.[I:6][CH2:7][CH2:8][OH:9].[C:10](=O)([O-])[O-].[K+].[K+]>P(Cl)(Cl)(Cl)=O>[CH3:1][O:2][C:3]([O:9][CH2:8][CH2:7][I:6])([CH3:4])[CH3:10]

Participants

5

Reactant 3

HCID 11430Potassium CarbonateHCID 12225IodoethanolHCID 1112901-Propene, 1-methoxy-

Product 1

HCID 19858315HCID 19858315, compound

Reagents, catalysts & solvents 1

HCID 24813Phosphorus oxychlorideCatalyst

Procedure

To 6 mls of cold (0° C.) methoxypropene was added 3 mls of 2-iodoethanol and 1 drop of phosphorous oxychloride (POCl3). The reaction was stirred for 1 hour and then solid potassium carbonate was added. After 10 minutes the liquid was decanted and concentrated to give the product as an oil.

Workup

  1. customAfter 10 minutes the liquid was decanted
  2. concentrationconcentrated

Sources & evidence

ORD record
ord-96a9a1d08ed443f8b99ee43952048400
Source dataset
uspto-grants-1989_04
Patent number
US04824849

Reaction notes

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