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HRID623974

反应详情

EQUATION

反应方程式

HRID 623974 的结构方程式

REACTANTS

反应物

2
结构：CNc1ccccc1
HCID7515

N-Methylaniline

C7H9N

结构：O=S(=O)([O-])C(F)(F)F.O=c1[nH]c2ccc(Br)cc2c(O)c1[I+]c1ccccc1
HCID86715456

未命名化合物

PRODUCTS

生成物

1
结构：CN(c1ccccc1)c1c(O)c2cc(Br)ccc2[nH]c1=O
HCID86715459

未命名化合物

PROCEDURE

实验过程

The title compound was prepared using N-methylaniline in place of aniline according to the procedure of Intermediate 11, step c except the crude solid was purified by flash column chromatography (silica gel, 50% EtOAc-Heptane), affording the title compound.

WORKUP

后处理

  1. customThe title compound was prepared
  2. customwas purified by flash column chromatography (silica gel, 50% EtOAc-Heptane)