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HRID624644

反应详情

EQUATION

反应方程式

HRID 624644 的结构方程式

REACTANTS

反应物

3
结构：CN(C)C(On1nnc2ccccc21)=[N+](C)C.F[P-](F)(F)(F)(F)F
HCID2733084

Methanaminium, N-[(1H-benzotriazol-1-yloxy)(dimethylamino)methylene]-N-methyl-, hexafluorophosphate(1-) (1:1)

C11H16F6N5OP

结构：O=C(O)c1cn2c(n1)-c1ccc(Br)cc1OCC2
HCID58204351

未命名化合物

结构：CC(N)=NNC(C)C
HCID74037752

未命名化合物

PRODUCTS

生成物

1
结构：CC(=NC(=O)c1cn2c(n1)-c1ccc(Br)cc1OCC2)NNC(C)C
HCID178464915

未命名化合物

AUXILIARIES

试剂、催化剂与溶剂

1
结构：CN(C)C=O
溶剂HCID6228

N,N-Dimethylformamide

C3H7NO

PROCEDURE

实验过程

Coupling of 28 with N′-isopropylacetohydrazonamide 6 and coupling reagent HBTU in DMF gives intermediate, 9-bromo-N-(1-(2-isopropylhydrazinyl)ethylidene)-5,6-dihydrobenzo[f]imidazo[1,2-d][1,4]oxazepine-2-carboxamide 34, which forms III upon heating.