huagongshe.com
HRID628094

反应详情

EQUATION

反应方程式

HRID 628094 的结构方程式

REACTANTS

反应物

3
结构：OO
HCID784

Hydrogen peroxide

H2O2

结构：O=C([O-])[O-].[K+].[K+]
HCID11430

Potassium Carbonate

CK2O3

结构：N#Cc1ccc2c(n1)-c1sc(-c3ncnn3-c3ccc(F)cc3F)cc1CCO2
HCID57900506

未命名化合物

PRODUCTS

生成物

1
结构：NC(=O)c1ccc2c(n1)-c1sc(-c3ncnn3-c3ccc(F)cc3F)cc1CCO2
HCID57900525

未命名化合物

收率 38%

AUXILIARIES

试剂、催化剂与溶剂

2
结构：CS(C)=O
溶剂HCID679

Dimethyl sulfoxide

C2H6OS

结构：O
溶剂HCID962

Water

H2O

PROCEDURE

实验过程

Following the procedure to prepare 379, compound 366, hydrogen peroxide, potassium carbonate in water and DMSO were reacted to give 432. Yield 38% MS: (ESI+)=426.1

WORKUP

后处理

  1. customwere reacted