huagongshe.com
HRID629840

反应详情

EQUATION

反应方程式

HRID 629840 的结构方程式

REACTANTS

反应物

4
结构：CI
HCID6328

Methyl iodide

CH3I

结构：BrCc1ccccc1
HCID7498

alpha-Bromotoluene

C7H7Br

结构：CC(C)(C)[C@@]1(C)OCO[C@]23CC[C@@]4(C[C@@H]21)[C@H]1Cc2ccc(O)c5c2[C@@]4(CCN1CC1CC1)[C@H]3O5
HCID73211769

未命名化合物

结构：CC(C)(C)[C@@]1(C)OCO[C@]23CC[C@@]4(C[C@@H]21)[C@H]1Cc2ccc(OCc5ccccc5)c5c2[C@@]4(CCN1CC1CC1)[C@H]3O5
HCID121278739

未命名化合物

PRODUCTS

生成物

1
结构：COc1ccc2c3c1O[C@H]1[C@@]45CC[C@]6(C[C@@H]4[C@@](C)(C(C)(C)C)OCO5)[C@@H](C2)N(C)CC[C@]316
HCID86711667

未命名化合物

收率 81.3%

PROCEDURE

实验过程

The title compound 23 was synthesized similar to the procedure described in Example 5 for preparing compound 7 using methyl iodide rather than benzyl bromide and compound 22 rather than compound 3. After column chromatography, 168 mg (81.3% yield) of compound 23 was isolated in a purity of >99% as a white solid.

WORKUP

后处理

  1. customThe title compound 23 was synthesized similar to the procedure