HRID632777

反应详情

EQUATION

反应方程式

HRID 632777 的结构方程式

AUXILIARIES

试剂、催化剂与溶剂

2

PROCEDURE

实验过程

A mixture of 3,3-dimethyl-1-(1-methyl-4-nitro-1H-pyrazol-3-yl)pyrrolidin-2-one (170 mg), 10% palladium-carbon (76 mg), THF (2 mL) and methanol (2 mL) was stirred at room temperature for 2 hr under hydrogen atmosphere. The reaction mixture was filtered through a membrane filter, and the filtrate was concentrated under reduced pressure to give the title compound (140 mg).

WORKUP

后处理

  1. filtrationThe reaction mixture was filtered through a membrane
  2. filtrationfilter
  3. concentrationthe filtrate was concentrated under reduced pressure