反应详情

The product from Example 60C (0.75 g, 1.979 mmol) and sodium thiomethoxide (0.139 g, 1.979 mmol) were combined in dimethylformamide (3.96 mL), stirred for 4 hours and partitioned into ethyl acetate and cold water. The organic layer was washed with saturated aqueous sodium chloride, dried (anhydrous Na2SO4), filtered, and concentrated to afford the title compound (0.66 g, 96%).

1. custompartitioned into ethyl acetate and cold water
2. washThe organic layer was washed with saturated aqueous sodium chloride
3. dry with materialdried (anhydrous Na2SO4)
4. filtrationfiltered
5. concentrationconcentrated