Potassium Carbonate → HCID 23137363, compound

HRID 633675Notes

Reaction equation

HRID 633675 reaction equation
[C:1]([N:3]=[C:4]([N:12]([CH2:19][CH:20]=[C:21]([CH3:23])[CH3:22])[CH2:13][C:14]([O:16][CH2:17][CH3:18])=[O:15])OC1C=CC=CC=1)#[N:2].[C:24]([O:28][C:29]([NH:31][CH:32]1[CH2:37][CH2:36][CH2:35][NH:34][CH2:33]1)=[O:30])([CH3:27])([CH3:26])[CH3:25].C(=O)([O-])[O-].[K+].[K+]>CN(C)C=O>[C:1]([N:3]=[C:4]([N:12]([CH2:19][CH:20]=[C:21]([CH3:22])[CH3:23])[CH2:13][C:14]([O:16][CH2:17][CH3:18])=[O:15])[N:34]1[CH2:35][CH2:36][CH2:37][CH:32]([NH:31][C:29]([O:28][C:24]([CH3:27])([CH3:26])[CH3:25])=[O:30])[CH2:33]1)#[N:2]

Participants

5

Reactant 3

HCID 11430Potassium CarbonateHCID 42330413-(Boc-amino)piperidineHCID 57514539HCID 57514539, compound

Product 1

HCID 23137363HCID 23137363, compound

Reagents, catalysts & solvents 1

HCID 6228DimethylformamideSolvent

Procedure

Prepared by reacting cyanimino-[N-(3-methyl-2-buten-1-yl)-N-(ethoxy-carbonylmethyl)-amino]-phenyloxy-methane with 3-(tert.-butyloxycarbonylamino)-piperidine in the presence of potassium carbonate in N,N-dimethylformamide at ambient temperature.

Workup

  1. customPrepared
  2. customat ambient temperature

Sources & evidence

ORD record
ord-ead4ae3fd22e4ca1a0ca8a927ee5c628
Source dataset
uspto-grants-2016_04
Patent number
US09321791B2

Reaction notes

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