2-Mercaptoethanol → HCID 86756480, compound
Reaction equation
[C:1]([Cl:12])(=[O:11])[C:2]1[CH:10]=[CH:9][C:5]([C:6]([Cl:8])=[O:7])=[CH:4][CH:3]=1.[SH:13][CH2:14][CH2:15][OH:16]>C(N(CC)CC)C>[SH:13][CH2:14][CH2:15][OH:16].[C:6]([Cl:8])(=[O:7])[C:5]1[CH:9]=[CH:10][C:2]([C:1]([Cl:12])=[O:11])=[CH:3][CH:4]=1Participants
4
Reactant 2
Product 1
Reagents, catalysts & solvents 1
Procedure
Next, in the mixing section 22, the vapor atmosphere of terephthaloyl chloride was cooled, and the introduced base particles were exposed thereto for 2 minutes. Consequently, a polymerization reaction, using as a catalyst triethylamine contained in the base particles, took place on the surface of the base particles between 2-mercaptoethanol and terephthaloyl chloride, forming a film of 2-mercaptoethanol-terephthaloyl chloride co-polymer.
Workup
- customConsequently, a polymerization reaction
Sources & evidence
- ORD record
- ord-159637ee4081470885723faa315fbc03
- Source dataset
- uspto-grants-2001_02
- Patent number
- US06194487B1
Reaction notes
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