Hydrochloric Acid → HCID 20256296, compound

HRID 637847Notes

Reaction equation

[Cl:1][C:2]1[CH:3]=[C:4]([CH:9]=[C:10]([Cl:12])[CH:11]=1)[O:5][CH2:6][CH2:7]Br.[CH2:13]([NH2:16])[CH2:14][CH3:15].Cl>>[ClH:1].[Cl:1][C:2]1[CH:3]=[C:4]([CH:9]=[C:10]([Cl:12])[CH:11]=1)[O:5][CH2:6][CH2:7][NH:16][CH2:13][CH2:14][CH3:15]

Participants

Reactant 3

HCID 313Hydrochloric Acid

HCID 7852Propylamine

HCID 222467761-(2-Bromoethoxy)-3,5-dichlorobenzene

Product 1

HCID 20256296HCID 20256296, compound

Procedure

The title compound was prepared by the method of Preparation 34 from 2-(3,5-dichlorophenoxy)-1-bromoethane, n-propylamine and hydrogen chloride. The free base was obtained as an oil. The hydrochloride salt melted at 185°-186° C.

Workup

customThe free base was obtained as an oil

Sources & evidence

ORD record: ord-df2146f0385b4fb7a87f558f0dcf69d5
Source dataset: uspto-grants-1985_12
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US04558155

Reaction notes

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