HRID64143
反应详情
EQUATION
反应方程式
REACTANTS
反应物
PRODUCTS
生成物
AUXILIARIES
试剂、催化剂与溶剂
PROCEDURE
实验过程
A solution of the compound of Example 164 (0.48 g, 0.91 mmol) in 6 N HCl (10 ml) was heated at 70° C. for 3 h. The mixture was quenched with NaHCO3 solution and extracted as in Example 1(d). The solvent was distilled off to afford the product in 27% yield (0.12 g).
WORKUP
后处理
- customThe mixture was quenched with NaHCO3 solution
- extractionextracted as in Example 1(d)
- distillationThe solvent was distilled off
- customto afford the product in 27% yield (0.12 g)