HRID64143

反应详情

EQUATION

反应方程式

HRID 64143 的结构方程式

AUXILIARIES

试剂、催化剂与溶剂

1

PROCEDURE

实验过程

A solution of the compound of Example 164 (0.48 g, 0.91 mmol) in 6 N HCl (10 ml) was heated at 70° C. for 3 h. The mixture was quenched with NaHCO3 solution and extracted as in Example 1(d). The solvent was distilled off to afford the product in 27% yield (0.12 g).

WORKUP

后处理

  1. customThe mixture was quenched with NaHCO3 solution
  2. extractionextracted as in Example 1(d)
  3. distillationThe solvent was distilled off
  4. customto afford the product in 27% yield (0.12 g)