HRID645475

反应详情

EQUATION

反应方程式

HRID 645475 的结构方程式

AUXILIARIES

试剂、催化剂与溶剂

1

PROCEDURE

实验过程

4-(3,3-difluoro-pyrrolidin-1-yl)-piperidine-1-carboxylic acid tert-butyl ester (1.77 mmol) is treated with 4N HCl in 1,4-dioxane (6 mL) and stirred at room temperature for 1 h. The reaction mixture is concentrated in vacuo and the resulting residue is used for the next step without further purification.

WORKUP

后处理

  1. concentrationThe reaction mixture is concentrated in vacuo
  2. customthe resulting residue is used for the next step without further purification