反应详情

A mixture of 4-bromophenol (30 g, 173 mmol), dibromoethane (40 mL, 464 mmol), NaOH (11.0 g, 275 mmol) and water (430 mL) was refluxed for 11 h. The phases were separated and the organic phase was further purified by distillation, yielding the sub-title compound (40.1 g 83%).

1. temperaturewas refluxed for 11 h
2. customThe phases were separated
3. distillationthe organic phase was further purified by distillation