Dodecylamine → HCID 86742100, compound

HRID 649063Notes

Reaction equation

HRID 649063 reaction equation
[C:1]([NH:4][C@@H:5]1[C@@H:11]([OH:12])[C@H:10]([OH:13])[C@@H:9]([CH2:14][OH:15])[O:8][CH:6]1O)(=[O:3])[CH3:2].[CH2:16]([NH2:28])[CH2:17][CH2:18][CH2:19][CH2:20][CH2:21][CH2:22][CH2:23][CH2:24][CH2:25][CH2:26][CH3:27]>C(O)C>[C:1]([NH:4][C@@H:5]1[C@@H:11]([OH:12])[C@H:10]([OH:13])[C@@H:9]([CH2:14][OH:15])[O:8][CH:6]1[CH2:27][CH2:26][CH2:25][CH2:24][CH2:23][CH2:22][CH2:21][CH2:20][CH2:19][CH2:18][CH2:17][CH2:16][NH2:28])(=[O:3])[CH3:2]

Participants

4

Reactant 2

HCID 13583DodecylamineHCID 439174N-Acetyl-D-Glucosamine

Product 1

HCID 86742100HCID 86742100, compound

Reagents, catalysts & solvents 1

HCID 702EthanolSolvent

Procedure

15 g of N-acetylglucosamine and 19 g of dodecylamine are heated at 80° C. for 3 hours in 50 ml of ethanol, with stirring. The undissolved material is then filtered off hot, the filtrate is cooled and the precipitated product is filtered off with suction and rinsed with ethanol and ether. The residue on the filter is dried in vacuo.

Workup

  1. filtrationThe undissolved material is then filtered off hot
  2. temperaturethe filtrate is cooled
  3. filtrationthe precipitated product is filtered off with suction
  4. washrinsed with ethanol and ether
  5. customThe residue on the filter is dried in vacuo

Sources & evidence

ORD record
ord-e985ae15e7b4405a8800e94f0ad0ca48
Source dataset
uspto-grants-1988_04
Patent number
US04737488

Reaction notes

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