Cyanuric chloride → HCID 87972777, compound
Reaction equation
C(N[CH:6]1[CH2:11][C:10]([CH3:13])([CH3:12])[N:9]([O:14][CH2:15][C:16]([OH:19])([CH3:18])[CH3:17])[C:8]([CH3:21])([CH3:20])[CH2:7]1)CCC.[N:22]1[C:29]([Cl:30])=[N:28][C:26]([Cl:27])=[N:25][C:23]=1Cl.C(=O)(O)[O-].[Na+]>>[OH:19][C:16]([CH3:17])([CH3:18])[CH2:15][O:14][N:9]1[C:8]([CH3:20])([CH3:21])[CH2:7][CH:6]([CH2:11][CH2:6][CH2:7][CH2:8][NH:9][C:23]2[N:22]=[C:29]([Cl:30])[N:28]=[C:26]([Cl:27])[N:25]=2)[CH2:11][C:10]1([CH3:12])[CH3:13]Participants
4
Procedure
The compound prepared in Example 23B is reacted with an equimolar amount of cyanuric chloride and sodium bicarbonate at 0° C. to give the title compound.
Sources & evidence
- ORD record
- ord-a1bf7ade644f4785842ed36d31566028
- Source dataset
- uspto-grants-2001_08
- Patent number
- US06271377B1
Reaction notes
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