反应详情

In the same manner as described in Example 13 by using (1RS, 3RS)-cis-1-cyclohexyl-3-hydroxymethyl-1,2,3,4-tetrahydro-β-carboline (569 mg) [J.A.C.S. 102, 6976 (1980)], triethylamine (405 mg), CS2 (304 mg), methyl iodide (568 mg) and dimethylsulfoxide (5 ml), there is prepared the title compound (490 mg, 65%) as white powder. NMR (CDCl3, δ): 2.63 (s, 3H, CSSCH3), Mass m/e: 374 (M+), 326 (M+ --CH3SH).