反应详情

In the same manner as described in Example 29 by using (3RS)-3-hydroxymethyl-1,2,3,4-tetrahydro-β-carboline (1.01 g), triethylamine (0.7 ml), CS2 (0.3 ml), 4-methoxybenzyl chloride (1.0 g) and dimethylsulfoxide (5 ml), there is prepared the title compound (1.41 g, 71%) as white powder, NMR (CDCl3 +DMSO-d6, δ): 4.52 (s, 2H, ##STR16## Mass m/e: 398 (M+), 244 (M+ -- ##STR17##