N-(2-Hydroxyethyl)ethylenediamine → HCID 218081, compound

HRID 653402Notes

Reaction equation

HRID 653402 reaction equation
OCCNCCN.[O:8]1[CH2:13][CH2:12][N:11]([CH2:14][CH2:15][NH2:16])[CH2:10][CH2:9]1.ClC1N=NC(C2C=CC=CC=2)=CC=1C.Cl[C:32]1[N:33]=[N:34][C:35]([C:39]2[CH:44]=[CH:43][C:42]([O:45][CH3:46])=[CH:41][CH:40]=2)=[CH:36][C:37]=1[CH3:38]>>[O:8]1[CH2:13][CH2:12][N:11]([CH2:14][CH2:15][NH:16][C:32]2[N:33]=[N:34][C:35]([C:39]3[CH:44]=[CH:43][C:42]([O:45][CH3:46])=[CH:41][CH:40]=3)=[CH:36][C:37]=2[CH3:38])[CH2:10][CH2:9]1

Participants

5

Reactant 4

HCID 8112N-(2-Hydroxyethyl)ethylenediamineHCID 1199993-Chloro-4-methyl-6-phenylpyridazineHCID 4082852-MorpholinoethylamineHCID 14450225HCID 14450225, compound

Product 1

HCID 218081HCID 218081, compound

Procedure

Operation is carried out as in Example 1, replacing the N-(2-hydroxy ethyl) ethylenediamine by an equivalent quantity of 2-morpholino ethylamine and the 3-chloro 4-methyl 6-phenyl pyridazine by a corresponding quantity of 3-chloro 4-methyl 6-(4-methoxy phenyl) pyridazine.

Sources & evidence

ORD record
ord-215658670bde4654aabd54e2fdbbbc96
Source dataset
uspto-grants-1987_06
Patent number
US04677106

Reaction notes

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