HRID659600

反应详情

EQUATION

反应方程式

HRID 659600 的结构方程式

AUXILIARIES

试剂、催化剂与溶剂

2

PROCEDURE

实验过程

Seventy (70) parts by mass of styrene, 30 parts by mass of acrylonitrile, 1.0 part by mass of calcium phosphate, 0.03 part by mass of “GAFAC GB520” (trade name, dispersing agent, TOHO Chemical Industry Co.,Ltd.), 0.6 part by mass of laurylperoxide, 1.0 part by mass of t-dodecylmercaptan, and 200 parts by mass of ion-exchanged water were charged in a stainless steel reactor equipped with an agitator. The temperature was elevated to 80° C. and polymerization was carried out for 6 hours to obtain a copolymer having an intrinsic viscosity of 0.6 dl/g (at 20° C. in N,N′-dimethylformamide) with 98% conversion.

WORKUP

后处理

  1. additionwere charged in a stainless steel reactor
  2. customequipped with an agitator
  3. customwas elevated to 80° C.
  4. custompolymerization
  5. customto obtain a copolymer