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HRID660765

反应详情

EQUATION

反应方程式

HRID 660765 的结构方程式

REACTANTS

反应物

2
结构：CC(C)(C)[O-].[K+]
HCID23665647

2-Methyl-2-propanol, potassium salt

C4H9KO

结构：COC(=O)CN(c1ccc(OCC(=O)OCC[Si](C)(C)C)cc1OCc1ccccc1)S(N)(=O)=O
HCID68840538

未命名化合物

PRODUCTS

生成物

1
结构：C[Si](C)(C)CCOC(=O)COc1ccc(N2CC(=O)NS2(=O)=O)c(OCc2ccccc2)c1
HCID68838475

未命名化合物

AUXILIARIES

试剂、催化剂与溶剂

1
结构：C1CCOC1
溶剂HCID8028

Tetrahydrofuran

C4H8O

2 次

PROCEDURE

实验过程

To a solution of methyl N-(aminosulfonyl)-N-(2-(benzyloxy)-4-{2-oxo-2-[2-(trimethylsilyl)ethoxy]ethoxy}phenyl)glycinate in THF is added potassium t-butoxide (1.1 equivalent) in THF dropwise. The mixture is stirred at RT for 18 h. The solvent is removed under reduced pressure to afford the title compound which is used directly in the next step.

WORKUP

后处理

  1. customThe solvent is removed under reduced pressure