反应详情

温度

80 °C

A mixture of EXAMPLE 2B (13 g) and lithium hydroxide hydrate (3.78 g) in dioxane (250 mL) and water (100 mL) at 95° C. was stirred for 16 hours and concentrated. The concentrate in water was heated at 80° C. and filtered. The filtrate was treated with 1M HCl (90 mL) and filtered.

1. concentrationconcentrated
2. concentrationThe concentrate in water
3. filtrationfiltered
4. additionThe filtrate was treated with 1M HCl (90 mL)
5. filtrationfiltered