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HRID66829

反应详情

EQUATION

反应方程式

HRID 66829 的结构方程式

REACTANTS

反应物

2
结构：Br
HCID260

Hydrogen Bromide

BrH

结构：CCCn1c(-c2ccc([N+](=O)[O-])cc2)c(C)c2cc(OCc3ccccc3)ccc21
HCID20529107

未命名化合物

PRODUCTS

生成物

1
结构：CCCn1c(-c2ccc([N+](=O)[O-])cc2)c(C)c2cc(O)ccc21
HCID20529108

未命名化合物

AUXILIARIES

试剂、催化剂与溶剂

1
结构：CC(=O)O
溶剂HCID176

Acetic Acid

C2H4O2

PROCEDURE

实验过程

Four grams (10 m mole) of 5-benzyloxy-3-methyl-2-(4-nitro-phenyl)-1-propyl-1H-indole and 40 ml of a saturated solution of hydrogen bromide in glacial acetic acid were refluxed for 20 minutes. After evaporation, the residue was purified by chromatography on silicagel (solvent: toluene/acetone (20:1)).

WORKUP

后处理

  1. customAfter evaporation
  2. customthe residue was purified by chromatography on silicagel (solvent: toluene/acetone (20:1))