Hydrogen Bromide → HCID 20527220, compound

HRID 67754Notes

Reaction equation

HRID 67754 reaction equation
Br.Br.[Cl:3][C:4]1[CH:9]=[CH:8][C:7]([C:10]2[N:11]([CH3:24])[C:12](=[N:15][C:16]3[CH:21]=[CH:20][C:19]([O:22][CH3:23])=[CH:18][CH:17]=3)[S:13][CH:14]=2)=[CH:6][C:5]=1[S:25](=[O:30])(=[O:29])[N:26]([CH3:28])[CH3:27].C(N(CC)CC)C>C(O)C>[Cl:3][C:4]1[CH:9]=[CH:8][C:7]([C:10]2[N:11]([CH3:24])[C:12](=[N:15][C:16]3[CH:17]=[CH:18][C:19]([O:22][CH3:23])=[CH:20][CH:21]=3)[S:13][CH:14]=2)=[CH:6][C:5]=1[S:25](=[O:30])(=[O:29])[N:26]([CH3:28])[CH3:27]

Participants

5

Reactant 3

HCID 260Hydrogen BromideHCID 8471TriethylamineHCID 20527350HCID 20527350, compound

Product 1

HCID 20527220HCID 20527220, compound

Reagents, catalysts & solvents 1

HCID 702EthanolSolvent

Procedure

Obtained by a procedure analogous to that indicated in Example 2 (a), from the hydrobromide of the title compound (Example 14) and triethylamine in ethanol. Colorless crystals; melting point 198°-199° C.

Workup

  1. customObtained by a procedure analogous to

Sources & evidence

ORD record
ord-ef83169b6d90462ab2387536195fd0fe
Source dataset
uspto-grants-1982_08
Patent number
US04346088

Reaction notes

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