Hydrogen Bromide → 4-(4-Chloro-3-dimethylsulfamoylphenyl)-3-methyl-2-(4-trifluoromethylphenyl-imino)-4-thiazoline

HRID 67755Notes

Reaction equation

HRID 67755 reaction equation
Br.Br.[Cl:3][C:4]1[CH:9]=[CH:8][C:7]([C:10]2[N:11]([CH3:26])[C:12](=[N:15][C:16]3[CH:21]=[CH:20][C:19]([C:22]([F:25])([F:24])[F:23])=[CH:18][CH:17]=3)[S:13][CH:14]=2)=[CH:6][C:5]=1[S:27](=[O:32])(=[O:31])[N:28]([CH3:30])[CH3:29]>C(N(CC)CC)C>[Cl:3][C:4]1[CH:9]=[CH:8][C:7]([C:10]2[N:11]([CH3:26])[C:12](=[N:15][C:16]3[CH:17]=[CH:18][C:19]([C:22]([F:24])([F:23])[F:25])=[CH:20][CH:21]=3)[S:13][CH:14]=2)=[CH:6][C:5]=1[S:27](=[O:31])(=[O:32])[N:28]([CH3:29])[CH3:30]

Participants

4

Reactant 2

HCID 260Hydrogen BromideHCID 205274154-(4-Chloro-3-dimethylsulfamoylphenyl)-3-methyl-2-(4-trifluoromethylphenyl-imino)-4-thiazoline hydrobromide

Product 1

HCID 205274164-(4-Chloro-3-dimethylsulfamoylphenyl)-3-methyl-2-(4-trifluoromethylphenyl-imino)-4-thiazoline

Reagents, catalysts & solvents 1

HCID 8471TriethylamineSolvent

Procedure

Obtained by a procedure analogous to that indicated in Example 2 (a), from the hydrobromide of the title compound of Example 16 and triethylamine. Melting point 147°-151° C.

Workup

  1. customObtained by a procedure analogous to

Sources & evidence

ORD record
ord-7700e3a46e8e4a09bfab84675735c503
Source dataset
uspto-grants-1982_08
Patent number
US04346088

Reaction notes

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