Dimethyl Sulfoxide → 4-Nitropicolinaldehyde

HRID 685330Notes

Reaction equation

HRID 685330 reaction equation
[CH3:22][CH2:23][N:24]([CH2:25][CH3:26])[CH2:27][CH3:28].[CH3:7][S:8](=[O:9])[CH3:10].[Cl:1][C:2]([C:3]([Cl:4])=[O:5])=[O:6].[Cl:29][CH2:30][Cl:31].[N+:11](=[O:12])([O-:13])[c:14]1[cH:15][c:16]([CH2:20][OH:21])[n:17][cH:18][cH:19]1>>[N+:11](=[O:12])([O-:13])[c:14]1[cH:15][c:16]([CH:20]=[O:21])[n:17][cH:18][cH:19]1

Participants

6

Reactant 5

HCID 679Dimethyl SulfoxideHCID 6344DichloromethaneHCID 8471TriethylamineHCID 65578Oxalyl chlorideHCID 14761455(4-Nitropyridin-2-yl)methanol

Product 1

HCID 145789294-Nitropicolinaldehyde

Sources & evidence

ORD record
ord-35d94c3a09da410fb6c6236356940426
Source dataset
Training data from https://doi.org/10.1039/C8SC04228D (3/10)

Reaction notes

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