反应详情

A mixture of acetic acid 1-oxo-5-[(R)-1-(tetrahydrofuran-2-yl)methoxy]-indan-2-yl ester (1.02 g) and potassium carbonate (264 mg) in methanol (1 mL) was stirred at room temperature for 1 h. After adding water it was extracted with dichloromethane, dried over magnesium sulfate and concentrated. In this way the product was obtained with molecular weight 248.28 (C14H16O4); MS (ESI): 249 (M+H+).

1. extractionwas extracted with dichloromethane
2. dry with materialdried over magnesium sulfate
3. concentrationconcentrated
4. customIn this way the product was obtained with molecular weight 248.28 (C14H16O4)