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HRID69871

反应详情

EQUATION

反应方程式

HRID 69871 的结构方程式

REACTANTS

反应物

3
结构：CCN(C(C)C)C(C)C
HCID81531

Diisopropylethylamine

C8H19N

结构：O=[N+]([O-])c1cc[n+]([O-])cc1Br
HCID548521

3-Bromo-4-nitropyridine N-oxide

C5H3BrN2O3

结构：CC(C)(C)OC(=O)NC1CCCNC1
HCID4233041

3-Boc-aminopiperidine

C10H20N2O2

PRODUCTS

生成物

1
结构：CC(C)(C)OC(=O)NC1CCCN(c2cnccc2[N+](=O)[O-])C1
HCID69046899

未命名化合物

收率 65%

PROCEDURE

实验过程

The method of Example 88 (Method 4) was followed using 1 eq each of 3-bromo-4-nitropyridine-N-oxide, 3-N-Boc-amino piperidine and diisopropylethylamine yielding tert-butyl 1-(4-nitropyridin-3-yl)piperidin-3-ylcarbamate (65%). LCMS (m/z): 339.1 (MH+); LC Rt=2.88 min.