Naphthalene → HCID 86639010, compound

HRID 71048Notes

Reaction equation

HRID 71048 reaction equation
[Na:1].[CH:2]1[C:11]2[C:6](=[CH:7][CH:8]=[CH:9][CH:10]=2)[CH:5]=[CH:4][CH:3]=1.[O:12]1[CH2:16][CH2:15][CH2:14][CH2:13]1>>[Na:1].[CH:10]1[C:11]2[C:6](=[CH:5][CH:4]=[CH:3][CH:2]=2)[CH:7]=[CH:8][CH:9]=1.[O:12]1[CH2:16][CH2:15][CH2:14][CH2:13]1

Participants

4

Reactant 3

HCID 931NaphthaleneHCID 8028TetrahydrofuranHCID 5360545Sodium

Product 1

HCID 86639010HCID 86639010, compound

Procedure

A complex reducing agent was prepared by reacting sodium (0.034 g/4.86 mmol) and naphthalene (0.622/4.86 mmol) in 70 ml of tetrahydrofuran under Ar flow in a 250 ml 1-neck round flask for 10 hours.

Workup

  1. customwas prepared
  2. customfor 10 hours

Sources & evidence

ORD record
ord-6183f732df1949c2a490b2e4ae7362c5
Source dataset
uspto-grants-2014_09
Patent number
US08822714B2

Reaction notes

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