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HRID712820

反应详情

EQUATION

反应方程式

HRID 712820 反应方程式

REACTANTS

反应物

3
1,3-Propanediamine, N'-(ethylcarbonimidoyl)-N,N-dimethyl-, monohydrochloride 分子结构式
HCID2723939

1,3-Propanediamine, N'-(ethylcarbonimidoyl)-N,N-dimethyl-, monohydrochloride

C8H18ClN3

Methyl 4-[(1S)-1-aminoethyl]benzoate--hydrogen chloride (1/1) 分子结构式
HCID57462942

Methyl 4-[(1S)-1-aminoethyl]benzoate--hydrogen chloride (1/1)

C10H14ClNO2

HCID 71187300 分子结构式
HCID71187300

未命名化合物

PRODUCTS

产物

1
HCID 117966958 分子结构式
HCID117966958

未命名化合物

收率 27.4%

PROCEDURE

实验过程

The title compound (D57) (25 mg) was prepared according to the general procedure for amides preparation (Method A) starting from 6-(tert-butoxycarbonyl)-5-methyl-6-azaspiro[2.5]octane-5-carboxylic acid (D6) (57 mg) and (S)-methyl 4-(1-aminoethyl)benzoate hydrochloride (46 mg). EDC.HCl: 1.1 eq, Reaction time: 48 hrs.

WORKUP

后处理

  1. custom48 hrs