HRID719445

反应详情

EQUATION

反应方程式

HRID 719445 的结构方程式

PROCEDURE

实验过程

To a portion of 6-chloro-N-(3-chloro-4-methoxyphenyl)-N′-cycloheptyl-[1,3,5]triazine-2,4-diamine (5 g) in isopropanol was added K2CO3 (3.2 g) and refluxed for about 10–12 h. TLC was monitored. After the completion of the reaction, the reaction mass was filtered through vacuum and the filtrate was evaporated to yield the title compound. (Wt. 3.7 g Y: 70%).

WORKUP

后处理

  1. temperaturerefluxed for about 10–12 h
  2. customAfter the completion of the reaction
  3. filtrationthe reaction mass was filtered through vacuum
  4. customthe filtrate was evaporated