HRID722207

反应详情

EQUATION

反应方程式

REACTANTS

反应物

结构：Cc1nnc(-c2ccccc2[N+](=O)[O-])n1-c1ccccc1C(=O)O

HCID21883887

2-[3-Methyl-5-(2-nitrophenyl)-4H-1,2,4-triazol-4-yl]benzoic acid

C16H12N4O4

PRODUCTS

生成物

HCID21883868

2-[3-(2-Aminophenyl)-5-methyl-4H-1,2,4-triazol-4-yl]benzoic acid

C16H14N4O2

AUXILIARIES

试剂、催化剂与溶剂

催化剂HCID23938

Palladium

溶剂HCID8028

Tetrahydrofuran

C4H8O

PROCEDURE

实验过程

was prepared by hydrogenating 400 mg of 2-[3-methyl-5-(2-nitrophenyl)-[1,2,4]triazol-4-yl]benzoic acid in the presence of Pd/C in tetrahydrofuran and purified by stirring with dichloromethane.

WORKUP

后处理

custompurified