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HRID722585

反应详情

EQUATION

反应方程式

HRID 722585 的结构方程式

REACTANTS

反应物

2
结构：Cc1ccc(S(=O)(=O)O)cc1.O
HCID521998

4-Methylbenzenesulfonic acid hydrate

C7H10O4S

结构：O=C(Nc1cc(Br)cc(F)c1O)c1cc([N+](=O)[O-])ccc1F
HCID21884296

未命名化合物

PRODUCTS

生成物

1
结构：O=[N+]([O-])c1ccc(F)c(-c2nc3cc(Br)cc(F)c3o2)c1
HCID21884570

未命名化合物

PROCEDURE

实验过程

Prepared by the method of Example 15b), from N-(2-hydroxy-3-fluoro-5-bromophenyl)-2-fluoro-5-nitrobenzamide (858 mg, 2.3 mmol) and p-toluenesulfonic acid monohydrate (961 g, 5.1 mmol) the subtitle compound was obtained (475 mg, 58%). 1H NMR (DMSO) δ 8.91(m, 1H), 8.57(m, 1H), 8.06(s, 1H), 7.81(m, 3H).