Indole → HCID 12995898, compound

HRID 722925Notes

Reaction equation

HRID 722925 reaction equation
[NH:1]1[C:9]2[C:4](=[CH:5][CH:6]=[CH:7][CH:8]=2)[CH:3]=[CH:2]1.[Cl:10][CH2:11][CH2:12][CH2:13][CH2:14][C:15](Cl)=[O:16]>>[Cl:10][CH2:11][CH2:12][CH2:13][CH2:14][C:15]([C:3]1[C:4]2[C:9](=[CH:8][CH:7]=[CH:6][CH:5]=2)[NH:1][CH:2]=1)=[O:16]

Participants

3

Reactant 2

HCID 798IndoleHCID 740895-Chlorovaleryl chloride

Product 1

HCID 12995898HCID 12995898, compound

Procedure

Using indole (1.00 g) and 5-chlorovaleryl chloride (1.68 ml) according to the same method as that of Reference Example 1, the title compound (1.55 g) was obtained as colorless crystals having a melting point of 165 to 167° C.

Sources & evidence

ORD record
ord-87b4ab8166854928a4303b6fb03e0fde
Source dataset
uspto-grants-2006_11
Patent number
US07138533B2

Reaction notes

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