Benzaldehyde → HCID 10997368, compound

Temperature

-74 °C

0.4 g (0.64 mmol) of the titanium compound prepared as in Example 4 are dissolved in 40 ml of diethyl ether, the solution is cooled to -74° C., 0.065 ml (0.65 mmol) of benzaldehyde are added and the mixture is stirred for 2 hours at -74° C. The reaction solution is then solution is then hydrolysed with 20 ml of aqueous ammonium fluoride solution, stirred overnight at RT, filtered through Hyflo and extracted with 3×40 ml of diethyl ether and the extract is washed with saturated NaCl solution, dried over Na2SO4 and evaporated.

1. filtrationfiltered through Hyflo
2. extractionextracted with 3×40 ml of diethyl ether
3. washthe extract is washed with saturated NaCl solution
4. dry with materialdried over Na2SO4
5. customevaporated

ORD record

ord-f72da6a1c32446aa9549a469ee47b1af

Source dataset

uspto-grants-1991_09

DOI

10.6084/m9.figshare.5104873.v1

Patent number

US05047557