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HRID730767

反应详情

EQUATION

反应方程式

HRID 730767 的结构方程式

REACTANTS

反应物

2
结构：O=P(Cl)(Cl)Cl
HCID24813

Phosphoric trichloride

Cl3OP

结构：O=c1[nH]c2cc(C(F)(F)F)cc([N+](=O)[O-])c2[nH]1
HCID11630155

未命名化合物

PRODUCTS

生成物

1
结构：O=[N+]([O-])c1cc(C(F)(F)F)cc2[nH]c(Cl)nc12
HCID11637534

未命名化合物

PROCEDURE

实验过程

The benzoimidazol-2-one from step (b) above (1.8 g, 7.3 mmol) reacted with POCl3 under the conditions of Example 1c to give the title compound as a yellow solid. MS (ESI, pos. ion) m/z: 266 (M+1).