反应详情

To 0.705 g (2.99 mmol) of the product of Example 19 in 15 mL of CH2Cl2 was added 1 g of solid NaHCO3 followed by 0.525 g (3.12 mmol) of allyl iodide. The reaction mixture was stirred overnight at room temperature, then filtered and evaporated in vacuo. The residue was purified on a silica gel flash chromatography column eluted with 0-1% MeOH in CH2Cl2. Evaporation of the purified fractions and drying in vacuo afforded the title compound.

1. filtrationfiltered
2. customevaporated in vacuo
3. customThe residue was purified on a silica gel flash chromatography column
4. washeluted with 0-1% MeOH in CH2Cl2
5. customEvaporation of the purified fractions
6. customdrying in vacuo