HRID734795

反应详情

EQUATION

反应方程式

REACTANTS

反应物

HCID69353

2,5-Dibromopyridine

C5H3Br2N

HCID18751415

未命名化合物

PRODUCTS

生成物

HCID69060371

未命名化合物

AUXILIARIES

试剂、催化剂与溶剂

溶剂HCID8857

Ethyl acetate

C4H8O2

PROCEDURE

实验过程

The product was obtained analogously to Example 1.1d starting from 7.70 g (47.48 mmol) of 2-(4-ethynylphenoxy)ethanol and 11.37 g (48.00 mmol) of 2,5-dibromopyridine. Yield: 7.40 g (49% of theoretical); C15H12BrNO2 (M=318.165); calc.: molpeak (M+H)+: 318/320 (Br); found: molpeak (M+H)+: 318/320 (Br); Rf value: 0.20 (silica gel, PE/EtOAc 6:4).

WORKUP

后处理

customThe product was obtained analogously to Example 1.1d