HRID734819

反应详情

EQUATION

反应方程式

REACTANTS

反应物

HCID61697

Bromine chloride (BrCl)

BrCl

2 次

HCID69381

Piperidine, 4-methyl-

C6H13N

结构：CS(=O)(=O)OCCOc1ccc(C#Cc2ncc(-c3ccc(Cl)cc3)cc2Br)cc1

HCID86601136

未命名化合物

PRODUCTS

生成物

结构：CC1CCN(CCOc2ccc(C#Cc3ncc(-c4ccc(Cl)cc4)cc3Br)cc2)CC1

HCID11598674

未命名化合物

PROCEDURE

实验过程

The product was obtained analogously to Example 7.1g starting from 2-{4-[3-bromo-5-(4-chlorophenyl)pyridin-2-ylethynyl]phenoxy}ethyl methanesulfonate and 4-methylpiperidine. Yield: 0.15 g (88% of theoretical); C27H26BrClN2O (M=509.865); calc.: molpeak (M+H)+: 509/511/513 (BrCl); found: molpeak (M+H)+: 509/511/513 (BrCl); HPLC-MS: 6.11 minutes (method A).

WORKUP

后处理

custom6.11 minutes (method A)