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HRID734822

反应详情

EQUATION

反应方程式

HRID 734822 的结构方程式

REACTANTS

反应物

2
结构：C#C[Si](C)(C)C
HCID66111

Trimethylsilylacetylene

C5H10Si

结构：Nc1cc(-c2ccc(Cl)cc2)cnc1Br
HCID85969704

未命名化合物

PRODUCTS

生成物

1
结构：C[Si](C)(C)C#CNc1cncc(-c2ccc(Cl)cc2)c1
HCID69059378

未命名化合物

PROCEDURE

实验过程

The product was obtained analogously to Example 7.1b starting from 2-bromo-5-(4-chlorophenyl)pyridin-3-ylamine (Example 16.1c) and trimethylsilylacetylene. Yield: 1.09 g (51% of theoretical); C16H17ClN2Si (M=300.858); calc.: molpeak (M+H)+: 301/303 (Cl); found: molpeak (M+H)+: 301/303 (Cl).

WORKUP

后处理

  1. customThe product was obtained analogously to Example 7.1b