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HRID734874

反应详情

EQUATION

反应方程式

HRID 734874 的结构方程式

REACTANTS

反应物

2
结构：C#C[Si](C)(C)C
HCID66111

Trimethylsilylacetylene

C5H10Si

结构：CN(C)c1cc(-c2ccc(Cl)cc2)cnc1Br
HCID86076948

未命名化合物

PRODUCTS

生成物

1
结构：CN(C)c1cc(-c2ccc(Cl)cc2)cnc1C#C[Si](C)(C)C
HCID69058189

未命名化合物

PROCEDURE

实验过程

The product was prepared analogously to Example 7.1c starting from [2-bromo-5-(4-chlorophenyl)pyridin-3-yl]dimethylamine and trimethylsilylacetylene. Yield: 0.50 g (quant. yield); C18H21ClN2Si (M=328.911); calc.: molpeak (M+H)+:329/331 (Cl); found: molpeak (M+H)+:329/331 (Cl); HPLC-MS: 7.41 minutes (method B).

WORKUP

后处理

  1. customThe product was prepared analogously to Example 7.1c
  2. custom7.41 minutes (method B)