Hydrochloric Acid → N-(1-methylimidazol-2-yl)benzylideneamine hydrochloride

HRID 741709Notes

Reaction equation

HRID 741709 reaction equation
[CH3:1][N:2]1[CH:6]=[CH:5][N:4]=[C:3]1[N:7]=[CH:8][C:9]1[CH:14]=[CH:13][CH:12]=[CH:11][CH:10]=1.[ClH:15].C(OCC)(=O)C>C(OCC)C>[ClH:15].[CH3:1][N:2]1[CH:6]=[CH:5][N:4]=[C:3]1[N:7]=[CH:8][C:9]1[CH:14]=[CH:13][CH:12]=[CH:11][CH:10]=1

Participants

5

Reactant 3

HCID 313Hydrochloric AcidHCID 8857Ethyl AcetateHCID 53843952N-(1-methylimidazol-2-yl)benzylideneamine

Product 1

HCID 67740815N-(1-methylimidazol-2-yl)benzylideneamine hydrochloride

Reagents, catalysts & solvents 1

HCID 3283Diethyl EtherSolvent

Procedure

N-(1-methylimidazol-2-yl)benzylideneamine (0.1 g) was dissolved in diethyl ether, and 4N hydrochloric acid--ethyl acetate (0.2 ml) was added. The precipitated pale yellow powder (70.mg, 21.9%) was separated by filtration.

Workup

  1. customThe precipitated pale yellow powder (70.mg, 21.9%) was separated by filtration

Sources & evidence

ORD record
ord-1e7072fc9e0845de90a53ef38b7a4328
Source dataset
uspto-grants-1996_09
Patent number
US05552427

Reaction notes

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