HRID743191
反应详情
EQUATION
反应方程式
REACTANTS
反应物
PRODUCTS
生成物
AUXILIARIES
试剂、催化剂与溶剂
PROCEDURE
实验过程
Following a procedure similar to that described in Example 1(c), 2 ml of a 4N solution of hydrogen chloride in dioxane were added to a solution of 0.29 g of 1-{2-[4-(3,5-dimethoxyphenyl)butyl]phenoxy}-3-dimethylamino-2-propanol [prepared as described in step (b) above] in ethyl acetate. The solvent was then removed by distillation under reduced pressure, and the resulting residue was dried in vacuo, to give 320 mg of the title compound as a colorless oil.
WORKUP
后处理
- customThe solvent was then removed by distillation under reduced pressure
- customthe resulting residue was dried in vacuo